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Subject: Exploring Accelerated Solvent Extraction and GC-MS/MS for Improved
 POP Analysis
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Accelerated Solvent Extraction and GC-MS Analysis of PCBs in Soil

Polychlorinated biphenyls (PCBs) are synthetic organic chlorinated hydrocar=
bons that have been used in hundreds of industrial and commercial applicati=
ons. Although now banned in the US due to their widespread toxicity, PCBs f=
ail to break down in the environment and instead cycle between air, water, =
and soil, entering the food chain and posing threats to animals and humans.=
 Current EPA-approved techniques for measuring PCBs in soil use Soxhlet ext=
raction techniques which are labor intensive and suffer from high solvent c=
onsumption, among other complications.

This application note demonstrates a method for the determination of PCBs i=
n soil using the new Thermo Scientific EXTREVA ASE Accelerated Solvent Extr=
actor upstream of analysis by GC-MS. This fully automated parallel extracto=
r and evaporator system is coupled with the Thermo Scientific TRACE 1310 Ga=
s Chromatograph and Thermo Scientific ISQ Single Quadrupole Mass Spectromet=
er for the determination of 17 PCBs in a range of soil matrices. Advantages=
 of this system include:

- Use of up to six different extraction solvents and up to four extraction =
cells in parallel
- Extraction and evaporation in one seamless operation with outstanding sam=
ple recovery and precision
- Carryover rates of less than 1% with minimal risk of sample cross-contami=
nation
- Excellent extraction efficiency, throughput, and performance to resolve c=
hallenging PCB applications

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<table role=3D"presentation" cellpadding=3D"0" cellspacing=3D"0" width=3D"1=
00%"><tbody><tr><td class=3D"hs_padded" style=3D"font-family:Georgia, serif=
; font-size:18px; color:#23286b; word-break:break-word; padding:10px 20px">=
<div id=3D"hs_cos_wrapper_module_16242852582431" class=3D"hs_cos_wrapper hs=
_cos_wrapper_widget hs_cos_wrapper_type_module" style=3D"color: inherit; fo=
nt-size: inherit; line-height: inherit;" data-hs-cos-general-type=3D"widget=
" data-hs-cos-type=3D"module"><div id=3D"hs_cos_wrapper_module_162428525824=
31_" class=3D"hs_cos_wrapper hs_cos_wrapper_widget hs_cos_wrapper_type_rich=
_text" style=3D"color: inherit; font-size: inherit; line-height: inherit;" =
data-hs-cos-general-type=3D"widget" data-hs-cos-type=3D"rich_text"><h1 styl=
e=3D"margin:0; mso-line-height-rule:exactly; font-family:Georgia, serif; co=
lor:#23286b; font-size:18px; line-height:125%; text-align:center" align=3D"=
center"><span style=3D"color: #000000; font-family: Arial, sans-serif;">Acc=
elerated Solvent Extraction and GC-MS Analysis of PCBs in Soil</span></h1>
<p style=3D"mso-line-height-rule:exactly; font-size:15px; line-height:125%"=
>&nbsp;</p>
<p style=3D"mso-line-height-rule:exactly; font-size:15px; line-height:125%"=
><span style=3D"color: #000000;"><span style=3D"font-family: Arial, sans-se=
rif;">Polychlorinated biphenyls (PCBs) are synthetic organic chlorinated hy=
drocarbons that have been used in hundreds of industrial and commercial app=
lications. Although now banned in the US due to their widespread toxicity, =
PCBs fail to break down in the environment and instead cycle between air, w=
ater, and soil, entering the food chain and posing threats to animals and h=
umans. Current EPA-approved techniques for measuring PCBs in soil use Soxhl=
et extraction techniques which are labor intensive and suffer from high sol=
vent consumption, among other complications.</span></span></p>
<p style=3D"mso-line-height-rule:exactly; font-size:15px; line-height:125%"=
>&nbsp;</p>
<p style=3D"mso-line-height-rule:exactly; font-size:15px; line-height:125%"=
><span style=3D"color: #000000;"><span style=3D"font-family: Arial, sans-se=
rif;">This application note demonstrates a method for the determination of =
PCBs in soil using the new Thermo Scientific EXTREVA ASE Accelerated Solven=
t Extractor upstream of analysis by GC-MS. This fully automated parallel ex=
tractor and evaporator system is coupled with the Thermo Scientific TRACE 1=
310 Gas Chromatograph and Thermo Scientific ISQ Single Quadrupole Mass Spec=
trometer for the determination of 17 PCBs in a range of soil matrices. Adva=
ntages of this system include:</span></span></p>
<ul style=3D"mso-line-height-rule:exactly; line-height:175%; list-style-typ=
e:circle">
<li style=3D"font-size: 15px; line-height: 125%;"><span style=3D"color: #00=
0000;"><span style=3D"font-family: Arial, sans-serif;">Use of up to six dif=
ferent extraction solvents and up to four extraction cells in parallel</spa=
n></span></li>
<li style=3D"font-size: 15px; line-height: 125%;"><span style=3D"color: #00=
0000;"><span style=3D"font-family: Arial, sans-serif;">Extraction and evapo=
ration in one seamless operation with outstanding sample recovery and preci=
sion</span></span></li>
<li style=3D"font-size: 15px; line-height: 125%;"><span style=3D"color: #00=
0000;"><span style=3D"font-family: Arial, sans-serif;">Carryover rates of l=
ess than 1% with minimal risk of sample cross-contamination</span></span></=
li>
<li style=3D"font-size: 15px; line-height: 125%;"><span style=3D"color: #00=
0000;"><span style=3D"font-family: Arial, sans-serif;">Excellent extraction=
 efficiency, throughput, and performance to resolve challenging PCB applica=
tions</span></span></li>
</ul></div></div></td></tr></tbody></table>
</div>


    
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